食品科学技术学报201601 - page 70

ricultural and Food Chemistry, 2006, 54 ( 7 ): 2695 -
2704.
[8]摇 FAN W L, QIAN M C. Identification of aroma com鄄
pounds in Chinese “ Yanghe Daqu 冶 liquor by normal
phase chromatography fractionation followed by gas chro鄄
matography / olfactometry [ J ]. Flavour and Fragrance
Journal, 2006,21(2):333 - 342.
[9]摇
王晓欣
,
徐岩
,
范文来
,
.
浓香型习酒挥发性香气成
分研究
[J].
酿酒科技
,2013,223(1): 31 - 37.
[10]摇
张会敏
,
束莹
,
周庆伍
,
.
利用非培养技术研究古井
贡酒大曲中的细菌群落结构
[ J].
现代食品科技
,
2014,30(4):44 - 49.
[11]摇
束莹
.
古井贡酒大曲中微生物群落结构的定性及分
[D].
哈尔滨
:
哈尔滨工业大学
,2013.
[12]摇
郭文杰
,
卢建春
.
古井贡酒特征香成分的研究
[ J].
酿酒科技
,2001,107(5):83 - 85.
[13]摇
黄艳梅
,
卢建春
,
李安军
.
采用气相色谱
-
质谱分析古井
贡酒中的风味物质
[J].
酿酒科技
,2006(7):91 -94.
[14]摇
张媛媛
,
孙金沅
,
张国锋
,
.
扳倒井芝麻香型白酒中
含硫风味成分的分析
[ J].
中国食品学报
,2012,12
(12): 173 - 179.
[15]摇
郑杨
,
赵纪文
,
张锋国
,
.
扳倒井芝麻香型白酒香成
分分析
[J].
食品科学
,2014,35(4):60 - 65.
[16]摇
王柏文
,
李贺贺
,
张锋国
,
.
应用液
-
液萃取结合
GC鄄
MS
GC鄄NPD
技术对国井芝麻香型白酒中含氮化合物
的分析
[J].
食品科学
,2014,35(10):126 -131.
[17]摇
孙啸涛
,
张锋国
,
董蔚
,
.
芝麻香白酒中
3鄄
甲硫基丙
醇的
GC鄄FPD
分析
[J].
食品科学技术学报
,2014,32
(5):27 - 34.
[18]摇 NIST. The NIST chemistry web book[EB / OL]. [2015鄄
03鄄16]. http: / / webbook. nist. gov / .
[19]摇 FANG Y, QIAN M. Aroma compounds in Oregon Pinot
Noir wine determined by aroma extract dilution analysis
(AEDA) [ J]. Flavour and Fragrance Journal,2005,20
(1):22 - 29.
[20]摇 LUO T, FAN W, XU Y. Characterization of volatile and
semi鄄volatile compounds in Chinese rice wines by head鄄
space solid phase microextraction followed by gas chro鄄
matography鄄mass spectrometry [J]. Journal of the Insti鄄
tute of Brewing, 2008,114(2):172 - 179.
[21]摇
张金修
,
李静
,
郭芳文
,
.
白酒中微量成分对人体的
作用
[J].
酿酒科技
,2014,244(10):143.
[22]摇 FAN W L, XU Y, ZHANG Y H. Characterization of
pyrazines in some Chinese liquors and their approximate
concentrations [ J ]. Journal of Agricultural and Food
Chemistry, 2007,55(24):9956 - 9962.
Research on Volatile Compounds in 2 Kinds of Gujinggong Liquor
LI Hehe
1
,摇 LIU Jinlong
1
,摇 LIANG Jinhui
2
,摇 GAO Jiangjing
2
,摇 SUN Jinyuan
1,*
,
HUANG Mingquan
1
,摇 ZHENG Fuping
1
,摇 SUN Baoguo
1
(1
. Beijing Laboratory for Food Quality and Safety / Beijing Key Laboratory of Flavor Chemistry
,
Beijing Technology and Business University
,
Beijing
100048,
China
;
2
. Gujinggong Group Co Ltd
,
Bozhou
236000,
China
)
Abstract
: The volatile compounds of Gujinggong liquor were analyzed by liquid鄄liquid extraction coupled
with GC鄄MS and identified by comparison with authentic standards, NIST 11 library and retention index.
Different compounds were extracted by using different organic solvents with various polarities. Compared
with diethyl ether and dichloromethane, n鄄pentane showed better extraction effect for aromatic com鄄
pounds; alkanes and sulfur鄄containing compounds, and dichloromethane showed better extraction effect
for heterocyclic compounds. A total of 188 volatile compounds were determined in Gujinggong liquor,
including 74 esters, 26 alcohols, 25 aromatic compounds, 20 acids, 14 alkanes, 8 aldehydes and ke鄄
tones, 8 sulfur鄄containing compounds, 7 acetals,4 heterocyclic compounds, and 2 lactone compounds.
About 167 compounds of them were identified by pure standard.
Key words
: liquid鄄liquid extraction; gas chromatography鄄mass spectrometry; Gujinggong liquor; volatile
compounds
(
责任编辑
:
)
56
34
卷 第
1
摇 摇 摇 摇 摇 摇 摇 摇 摇 摇
李贺贺等
: 2
种古井贡酒中挥发性成分的研究
1...,60,61,62,63,64,65,66,67,68,69 71,72,73,74,75,76,77,78,79,80,...84
Powered by FlippingBook